Determination of radium-226 in aqueous solutions by alpha-spectrometry

Anal Chem. 2001 Sep 1;73(17):4218-24. doi: 10.1021/ac0015220.

Abstract

The new European legislation imposes a lower threshold for radioactivity in drinking water. This requires the development of more sensitive and reliable analytical methods. This work presents an improved alpha-spectrometric technique to determine the radium-226 activity in aqueous solution relying on the radium adsorption onto a thin manganese oxide layer followed by alpha-measurement. The preparation of the MnO2 deposit has been optimized as well as the radium adsorption conditions. Detection threshold and limit of 5 and 10 mBq x L(-1), respectively, with a 10% (95% confidence) uncertainty are currently reached. This paper reports on the overall technique and on its application to assess the radium-226 activity in 28 French mineral waters. In addition, the gross alpha- and beta-activities have been evaluated using proportional counting while the uranium concentrations were derived from ICPMS.

MeSH terms

  • Algorithms
  • Alpha Particles
  • France
  • Manganese Compounds / chemistry
  • Oxides / chemistry
  • Radium / analysis*
  • Spectrum Analysis
  • Water Pollutants, Radioactive / analysis*
  • Water Supply / analysis*
  • Water Supply / standards

Substances

  • Manganese Compounds
  • Oxides
  • Water Pollutants, Radioactive
  • manganese oxide
  • Radium