Role of the N-terminal hydrophilic domain of acyl-coenzyme A:cholesterol acyltransferase 1 on the enzyme's quaternary structure and catalytic efficiency

Biochemistry. 2002 Mar 19;41(11):3762-9. doi: 10.1021/bi0120188.

Abstract

Acyl-coenzyme A:cholesterol acyltransferase (ACAT) is an enzyme involved in cellular cholesterol homeostasis and atherosclerosis. ACAT1 is an allosteric enzyme responding to its substrate cholesterol in a sigmoidal manner. It is a homotetrameric protein that spans the membrane multiple times, with its N-terminal 131 hydrophilic amino acids residing at the cytoplasmic side of the endoplasmic reticulum. This region contains two closely linked putative alpha-helices. Our current studies show that this region contains a dimer-forming motif. Adding this motif to the bacterial glutathione S-transferase (GST) converted the homodimeric GST to a tetrameric fusion protein. Conversely, deleting this motif from the full-length ACAT1 converted the enzyme from a homotetramer to a homodimer. The dimeric ACAT1 remains enzymatically active. Its biochemical characteristics, including the sigmoidal response to cholesterol, the IC(50) value toward a specific ACAT inhibitor, and sensitivity toward heat inactivation, are essentially unaltered. On the other hand, the dimeric ACAT1 exhibits a 5-10-fold increase in the V(max) of the overall reaction and a 2.2-fold increase in the K(m) for oleoyl-coenzyme. Thus, deleting the dimer-forming motif near the N-terminus changes ACAT1 from its tetrameric form to a dimeric form and increases its catalytic efficiency.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Allosteric Regulation
  • Amino Acid Sequence
  • Base Sequence
  • Catalysis
  • DNA Primers
  • Glutathione Transferase / metabolism
  • Hot Temperature
  • Molecular Sequence Data
  • Mutagenesis, Site-Directed
  • Protein Structure, Quaternary
  • Recombinant Fusion Proteins / metabolism
  • Sterol O-Acyltransferase / antagonists & inhibitors
  • Sterol O-Acyltransferase / chemistry
  • Sterol O-Acyltransferase / genetics
  • Sterol O-Acyltransferase / metabolism*

Substances

  • DNA Primers
  • Recombinant Fusion Proteins
  • Sterol O-Acyltransferase
  • Glutathione Transferase