Three-dimensional single molecule rotational diffusion in glassy state polymer films

Phys Rev Lett. 2002 Jul 8;89(2):026101. doi: 10.1103/PhysRevLett.89.026101. Epub 2002 Jun 24.

Abstract

Measuring three-dimensional orientational motions of many individual molecules within glassy state poly(methyl methacrylate) has enabled nanoscopic probing of bulk-obscured polymer dynamics. Complementing bulk studies, the measured distributions of nanoscale barriers to rotational motion afforded by our single molecule orientational methods directly probe the spatial heterogeneity and nanoscopic alpha-relaxation dynamics deep within the glassy state.