Optimization of peptide linker length in production of MHC class II/peptide tetrameric complexes increases yield and stability, and allows identification of antigen-specific CD4+T cells in peripheral blood mononuclear cells

Eur J Immunol. 2002 Dec;32(12):3366-75. doi: 10.1002/1521-4141(200212)32:12<3366::AID-IMMU3366>3.0.CO;2-#.

Abstract

Reliable, efficient systems for producing soluble HLA-DR molecules, suitable for multimerization and use as staining reagents, have proved elusive. We found that the addition of a flexible linker between peptide and N terminus of the DRB1*0101-chain (Crawford, F., Kozono, H., White, J., Marrack, P. and Kappler, J., Immunity 1998. 8: 675-682.), results in greater in vitro folding efficiency of Escherichia coli-expressed alpha- and beta-chains, and increases both the yield and stability of the DRA1*0101/DRB1*0101/peptide complexes. Although a 10-amino acid linker functioned efficiently for a 20mer epitope from HIV p24, a longer linker was required to produce a DR1 MHC class II tetramer with the influenza hemagglutinin epitope (HA(306-318)). The DR1-HA tetramer was able to stain positively over 98% of a specific clone (HA 1.7) with only a brief 30-min incubation. The tetrameric complexes detected clone cells diluted into PBMC, with high sensitivity, coupled with low background staining in CD4(+) cells. It was possible to detect antigen-specific CD4(+) T cells within a population of PBMC stimulated with the HA peptide. This demonstrates the potential to monitor CD4(+) T cell responses in peripheral blood in a number of clinical scenarios.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • CD4-Positive T-Lymphocytes / immunology*
  • Clone Cells
  • Flow Cytometry
  • HLA-DR Antigens / chemistry*
  • HLA-DR Antigens / isolation & purification
  • HLA-DR Serological Subtypes
  • HLA-DR1 Antigen / chemistry*
  • HLA-DR1 Antigen / isolation & purification
  • Humans
  • Interferon-gamma / metabolism
  • Leukocytes, Mononuclear / immunology
  • Macromolecular Substances
  • Staining and Labeling

Substances

  • HLA-DR Antigens
  • HLA-DR Serological Subtypes
  • HLA-DR1 Antigen
  • HLA-DR11 antigen
  • Macromolecular Substances
  • Interferon-gamma