The N-terminal domain of p53 is natively unfolded

J Mol Biol. 2003 Oct 3;332(5):1131-41. doi: 10.1016/j.jmb.2003.08.008.

Abstract

p53 is one of the key molecules regulating cell proliferation, apoptosis and tumor suppression by integrating a wide variety of signals. The structural basis for this function is still poorly understood. p53 appears to exercise its function as a modular protein in which different functions are associated with distinct domains. Presumably, p53 contains both folded and partially structured parts. Here, we have investigated the structure of the isolated N-terminal part of p53 (amino acid residues 1-93) using biophysical techniques. We demonstrate that this domain is devoid of tertiary structure and largely missing secondary structure elements. It exhibits a large hydrodynamic radius, typical for unfolded proteins. These findings suggest strongly that the entire N-terminal part of p53 is natively unfolded under physiological conditions. Furthermore, the binding affinity to its functional antagonist Mdm2 was investigated. A comparison of the binding of human Mdm2 to the N-terminal part of p53 and full-length p53 suggests that unfolded and folded parts of p53 function synergistically.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Apoptosis
  • Biophysical Phenomena
  • Biophysics
  • Cell Division
  • Chromatography, Gel
  • Circular Dichroism
  • Humans
  • Magnetic Resonance Spectroscopy
  • Nuclear Proteins*
  • Plasmids / metabolism
  • Protein Binding
  • Protein Folding
  • Protein Structure, Quaternary
  • Protein Structure, Secondary
  • Protein Structure, Tertiary
  • Proto-Oncogene Proteins / chemistry
  • Proto-Oncogene Proteins c-mdm2
  • Spectrometry, Fluorescence
  • Tumor Suppressor Protein p53 / chemistry*
  • Ultracentrifugation
  • Water / chemistry

Substances

  • Nuclear Proteins
  • Proto-Oncogene Proteins
  • Tumor Suppressor Protein p53
  • Water
  • MDM2 protein, human
  • Proto-Oncogene Proteins c-mdm2