Development of an epitope tag for the gentle purification of proteins by immunoaffinity chromatography: application to epitope-tagged green fluorescent protein

Anal Biochem. 2003 Dec 15;323(2):171-9. doi: 10.1016/j.ab.2003.08.003.

Abstract

Polyol-responsive monoclonal antibodies (mAbs) are useful tools for the gentle purification of proteins and protein complexes. These are high-affinity mAbs that release the antigen in the presence of a nonchaotropic salt and a low-molecular-weight polyhydroxylated compound (polyol). The epitope for the polyol-responsive mAb NT73, which reacts with Escherichia coli RNA polymerase, was located at the C terminus of the beta' subunit. Using recombinant DNA techniques, we have identified the epitope to be within the 13-amino-acid sequence SLAELLNAGLGGS and have developed an epitope tag that can be fused to a protein of interest for use as a purification tag. This epitope tag (designated Softag1) was fused to either the N or the C terminus of the green fluorescent protein. These tagged proteins were expressed in E. coli, and the tagged proteins were purified from the soluble fraction by a single-step immunoaffinity chromatography procedure. This approach extends the powerful technique of gentle-release immunoaffinity chromatography to many expressed proteins.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Antibodies, Monoclonal / immunology
  • Antibody Specificity
  • Chromatography, Affinity*
  • Enzyme-Linked Immunosorbent Assay
  • Epitope Mapping
  • Epitopes / genetics
  • Epitopes / immunology
  • Epitopes / isolation & purification*
  • Escherichia coli
  • Green Fluorescent Proteins
  • Immunologic Techniques
  • Luminescent Proteins / genetics
  • Luminescent Proteins / isolation & purification*
  • Molecular Sequence Data
  • Polymers / pharmacology

Substances

  • Antibodies, Monoclonal
  • Epitopes
  • Luminescent Proteins
  • Polymers
  • polyol
  • Green Fluorescent Proteins