Potent pyrimidinetrione-based inhibitors of MMP-13 with enhanced selectivity over MMP-14

Bioorg Med Chem Lett. 2005 Apr 1;15(7):1807-10. doi: 10.1016/j.bmcl.2005.02.038.

Abstract

Through the use of computational modeling, a series of pyrimidinetrione-based inhibitors of MMP-13 was designed based on a lead inhibitor identified through file screening. Incorporation of a biaryl ether moiety at the C-5 position of the pyrimidinetrione ring resulted in a dramatic enhancement of MMP-13 potency. Protein crystallography revealed that this moiety binds in the S(1)(') pocket of the enzyme. Optimization of the C-4 substituent of the terminal aromatic ring led to incorporation of selectivity versus MMP-14 (MT-1 MMP). Structure activity relationships of the biaryl ether substituent are presented as is pharmacokinetic data for a compound that meets our in vitro potency and selectivity goals.

MeSH terms

  • Binding Sites
  • Collagenases / chemistry
  • Crystallography, X-Ray
  • Enzyme Inhibitors / chemical synthesis*
  • Enzyme Inhibitors / pharmacology
  • Matrix Metalloproteinase 13
  • Matrix Metalloproteinase Inhibitors*
  • Pyrimidines / chemistry*
  • Structure-Activity Relationship

Substances

  • Enzyme Inhibitors
  • Matrix Metalloproteinase Inhibitors
  • Pyrimidines
  • Collagenases
  • Matrix Metalloproteinase 13