Multi-step fibrinogen binding to the integrin (alpha)IIb(beta)3 detected using force spectroscopy

Biophys J. 2005 Oct;89(4):2824-34. doi: 10.1529/biophysj.105.061887. Epub 2005 Jul 22.

Abstract

The regulated ability of integrin alphaIIbbeta3 to bind fibrinogen plays a crucial role in platelet aggregation and hemostasis. We have developed a model system based on laser tweezers, enabling us to measure specific rupture forces needed to separate single receptor-ligand complexes. First of all, we performed a thorough and statistically representative analysis of nonspecific protein-protein binding versus specific alphaIIbbeta3-fibrinogen interactions in combination with experimental evidence for single-molecule measurements. The rupture force distribution of purified alphaIIbbeta3 and fibrinogen, covalently attached to underlying surfaces, ranged from approximately 20 to 150 pN. This distribution could be fit with a sum of an exponential curve for weak to moderate (20-60 pN) forces, and a Gaussian curve for strong (>60 pN) rupture forces that peaked at 80-90 pN. The interactions corresponding to these rupture force regimes differed in their susceptibility to alphaIIbbeta3 antagonists or Mn2+, an alphaIIbbeta3 activator. Varying the surface density of fibrinogen changed the total binding probability linearly >3.5-fold but did not affect the shape of the rupture force distribution, indicating that the measurements represent single-molecule binding. The yield strength of alphaIIbbeta3-fibrinogen interactions was independent of the loading rate (160-16,000 pN/s), whereas their binding probability markedly correlated with the duration of contact. The aggregate of data provides evidence for complex multi-step binding/unbinding pathways of alphaIIbbeta3 and fibrinogen revealed at the single-molecule level.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Binding Sites
  • Elasticity
  • Fibrinogen / analysis*
  • Fibrinogen / chemistry*
  • Fibrinogen / ultrastructure
  • Lasers*
  • Microscopy, Atomic Force / methods*
  • Multiprotein Complexes / analysis
  • Multiprotein Complexes / chemistry
  • Platelet Glycoprotein GPIIb-IIIa Complex / analysis*
  • Platelet Glycoprotein GPIIb-IIIa Complex / chemistry*
  • Platelet Glycoprotein GPIIb-IIIa Complex / ultrastructure
  • Protein Binding
  • Spectrum Analysis / methods*
  • Stress, Mechanical

Substances

  • Multiprotein Complexes
  • Platelet Glycoprotein GPIIb-IIIa Complex
  • Fibrinogen