Determination of 1-furan-2-yl-3-pyridin-2-yl-propenone, an anti-inflammatory propenone compound, by high performance liquid chromatography with ultraviolet spectrometry

J Chromatogr B Analyt Technol Biomed Life Sci. 2006 Jun 6;837(1-2):108-11. doi: 10.1016/j.jchromb.2006.04.010. Epub 2006 May 9.

Abstract

1-Furan-2-yl-3-pyridin-2-yl-propenone (FPP-3) has recently been synthesized and characterized to have an anti-inflammatory activity. In the present study, pharmacokinetic parameters for FPP-3 and its metabolites were determined at the same time by using high-performance liquid chromatography-ultraviolet spectrometry. Two metabolites were detected in sera when FPP-3 was administered intravenously to male SD rats. The linearity of FPP-3, M1 (1-furan-2-yl-3-pyridin-2-yl-propan-1-one) and M2 (1-furan-2-yl-3-pyridin-2-yl-propan-1-ol) was confirmed in the concentration ranges of 0.5-20, 0.101-4.04 and 1.04-20.4 microg/ml, respectively. The lower limits of quantitation of FPP-3, M1 and M2 were 0.5, 0.1 and 1.0 microg/ml, respectively. The intra- and inter-day precision and accuracy over the concentration range of target compounds were within 13.5 and 14.2%, respectively. The half-lives of FPP-3, M1 and M2 were 16.3, 27.7 and 22.1 min, respectively.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Anti-Inflammatory Agents / blood*
  • Anti-Inflammatory Agents / pharmacokinetics
  • Chromatography, High Pressure Liquid / methods*
  • Furans / blood*
  • Furans / pharmacokinetics
  • Male
  • Propane / analogs & derivatives*
  • Propane / blood
  • Propane / pharmacokinetics
  • Pyridines / blood*
  • Pyridines / pharmacokinetics
  • Rats
  • Rats, Sprague-Dawley
  • Reproducibility of Results
  • Sensitivity and Specificity
  • Spectrophotometry, Ultraviolet / methods*

Substances

  • 1-furan-2-yl-3-pyridin-2-yl-propenone
  • Anti-Inflammatory Agents
  • Furans
  • Pyridines
  • Propane