Rapid validation of protein identifications with the borderline statistical confidence via de novo sequencing and MS BLAST searches

J Proteome Res. 2006 Sep;5(9):2448-56. doi: 10.1021/pr060200v.

Abstract

Protein identifications with the borderline statistical confidence are typically produced by matching a few marginal quality MS/MS spectra to database peptide sequences and represent a significant bottleneck in the reliable and reproducible characterization of proteomes. Here, we present a method for rapid validation of borderline hits that circumvents the need in, often biased, manual inspection of raw MS/MS spectra. The approach takes advantage of the independent interpretation of corresponding MS/MS spectra by PepNovo de novo sequencing software followed by mass spectrometry-driven BLAST (MS BLAST) sequence-similarity database searches that utilize all partially inaccurate, degenerate and redundant candidate peptide sequences. In a case study involving the identification of more than 180 Caenorhabditis elegans proteins by nanoLC-MS/MS analysis on a linear ion trap LTQ mass spectrometer, the approach enabled rapid assignment (confirmation or rejection) of more than 70% of Mascot hits of borderline statistical confidence.

Publication types

  • Comparative Study
  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Caenorhabditis elegans Proteins / analysis*
  • Caenorhabditis elegans Proteins / isolation & purification
  • Computational Biology / methods*
  • Mass Spectrometry / methods
  • Molecular Sequence Data
  • Proteomics / methods*
  • Sequence Analysis, Protein / methods*

Substances

  • Caenorhabditis elegans Proteins