Validation of incorporating flurbiprofen into the Pittsburgh cocktail

Clin Pharmacol Ther. 2006 Sep;80(3):257-63. doi: 10.1016/j.clpt.2006.06.005.

Abstract

Background: We have previously shown that flurbiprofen metabolism to 4'-hydroxyflurbiprofen provides an in vivo measure of cytochrome P450 (CYP) 2C9 activity. This study evaluated the possibility of incorporating flurbiprofen into the current 5-drug Pittsburgh cocktail.

Methods: In a randomized, 3-way, Latin-square, crossover-design study, 24 healthy subjects (mean age [+/-SD], 47.8 +/- 15.1 years) received flurbiprofen (50 mg) and the Pittsburgh 5-drug cocktail (100 mg caffeine, 100 mg mephenytoin, 10 mg debrisoquin [INN, debrisoquine], 250 mg chlorzoxazone, and 100 mg dapsone) separately and in combination on 3 occasions over a period of 5 weeks. Urine was collected from 0 to 8 hours, and plasma was obtained at 4 and 8 hours after drug administration. Parent drug and metabolite concentrations were measured to determine phenotypic indices for each of the metabolizing enzymes.

Results: The geometric mean ratio and 90% confidence interval of the phenotypic indices were included within the 80% to 125% bioequivalence range for each of the probe drugs. There were no statistically significant differences between the phenotypic indices determined after administration of the 5-drug and 6-drug cocktails. However, there was a small but statistically significant increase (7.5%, P = .03) in the 8-hour urinary flurbiprofen recovery ratio after administration of the 6-drug cocktail compared with that after administration of flurbiprofen alone. The 6-drug cocktail was well tolerated.

Conclusion: The results of this study show that caffeine (CYP1A2), chlorzoxazone (CYP2E1), dapsone (N-acetyltransferase 2), debrisoquin (CYP2D6), flurbiprofen (CYP2C9), and mephenytoin (CYP2C19) can be simultaneously administered in low doses without metabolic interaction.

Publication types

  • Comparative Study
  • Randomized Controlled Trial
  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.
  • Validation Study

MeSH terms

  • Administration, Oral
  • Adolescent
  • Adult
  • Aged
  • Caffeine / metabolism
  • Caffeine / pharmacology
  • Caffeine / therapeutic use
  • Chlorzoxazone / metabolism
  • Chlorzoxazone / pharmacology
  • Chlorzoxazone / therapeutic use
  • Cross-Over Studies*
  • Cytochrome P-450 Enzyme System / genetics
  • Cytochrome P-450 Enzyme System / metabolism
  • Dapsone / metabolism
  • Dapsone / pharmacology
  • Dapsone / therapeutic use
  • Debrisoquin / metabolism
  • Debrisoquin / pharmacology
  • Debrisoquin / therapeutic use
  • Drug Therapy, Combination
  • Female
  • Flurbiprofen / metabolism
  • Flurbiprofen / pharmacology*
  • Flurbiprofen / therapeutic use
  • Genotype
  • Humans
  • Isoenzymes / genetics
  • Isoenzymes / metabolism
  • Male
  • Mephenytoin / metabolism
  • Mephenytoin / pharmacology
  • Mephenytoin / therapeutic use
  • Middle Aged

Substances

  • Isoenzymes
  • Caffeine
  • Flurbiprofen
  • Dapsone
  • Cytochrome P-450 Enzyme System
  • Chlorzoxazone
  • Mephenytoin
  • Debrisoquin