Optical analysis of the HIF-1 complex in living cells by FRET and FRAP

FASEB J. 2007 Mar;21(3):700-7. doi: 10.1096/fj.06-6280com. Epub 2006 Dec 28.

Abstract

Hypoxia-inducible factor-1 (HIF-1) coordinates the cellular response to a lack of oxygen by controlling the expression of hypoxia-inducible genes that ensure an adequate energy supply. Assembly of the HIF-1 complex by its oxygen-regulated subunit HIF-1alpha and its constitutive beta subunit also known as ARNT is the key event of the cellular genetic response to hypoxia. By two-photon microscopy, we studied HIF-1 assembly in living cells and the mobility of fluorophore-labeled HIF-1 subunits by fluorescence recovery after photobleaching. We found a significantly slower nuclear migration of HIF-1alpha than of HIF-1beta, indicating that each subunit can move independently. We applied fluorescence resonance energy transfer to calculate the nanometer distance between alpha and beta subunits of the transcriptionally active HIF-1 complex bound to DNA. Both N termini of the fluorophore-labeled HIF-1 subunits were localized as close as 6.2 nm, but even the N and C terminus of the HIF-1 complex were not further apart than 7.4 nm. Our data suggest a more compact 3-dimensional organization of the HIF complex than described so far by 2-dimensional models.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Fluorescence Recovery After Photobleaching / methods*
  • Fluorescence Resonance Energy Transfer / methods*
  • Humans
  • Hypoxia-Inducible Factor 1, alpha Subunit / analysis*
  • Hypoxia-Inducible Factor 1, alpha Subunit / chemistry
  • Protein Subunits / analysis
  • Tumor Cells, Cultured

Substances

  • HIF1A protein, human
  • Hypoxia-Inducible Factor 1, alpha Subunit
  • Protein Subunits