A myoglobin functional model composed of a ferrous porphyrin and a cyclodextrin dimer with an imidazole linker

Chem Asian J. 2006 Sep 18;1(3):358-66. doi: 10.1002/asia.200600070.

Abstract

A 1:1 inclusion complex (Fe(II)PImCD) of 5,10,15,20-tetrakis- (4-sulfonatophenyl)porphinatoiron(II) (Fe(II)P) and an O-methylated beta-cyclodextrin dimer with an imidazole linker (ImCD) was found to bind dioxygen in aqueous solution. The half-saturation pressure of dioxygen (P(1/2)O2) is 1.7 torr at 25 degrees C, which is 10 times lower than that for a previous myoglobin functional model (hemoCD) with a pyridine linker. Meanwhile, the half-life of oxygenated Fe(II)PImCD is 3 h, which is 10 times shorter than that of oxygenated hemoCD. The covering of the iron(II) center by a microscopic environment is essential for preventing autoxidation of oxygenated ferrous porphyrin, which is promoted by nucleophilic attack of H2O and/or nucleophiles such as inorganic anions. Due to structural requirements, covering of the Fe(II) center of Fe(II)PImCD is insufficient compared with the case of hemoCD. As a result, water molecules can penetrate more easily the cleft of the O2-Fe(II)PImCD complex and act as an autoxidation inducer. This structure also causes poorer selectivity against carbon monoxide (M = 1040). In contrast, the dioxygen affinity of Fe(II)PImCD is much higher than that of hemoCD because the imidazole moiety is a stronger electron donor than pyridine.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Carbon / chemistry
  • Carbon Monoxide / chemistry
  • Chemistry, Pharmaceutical / methods
  • Cyclodextrins / chemistry*
  • Dimerization
  • Hemeproteins / chemistry*
  • Humans
  • Imidazoles / chemistry*
  • Metalloporphyrins / chemistry*
  • Myoglobin / chemistry*
  • Oxygen / chemistry
  • Oxygen / metabolism
  • Pyridines / chemistry
  • Temperature

Substances

  • Cyclodextrins
  • Hemeproteins
  • Imidazoles
  • Metalloporphyrins
  • Myoglobin
  • Pyridines
  • ferroporphyrin
  • Carbon
  • imidazole
  • Carbon Monoxide
  • pyridine
  • Oxygen