Unprecedented hydrogen transfer from water to alkenes and alkynes mediated by TiIII and late transition metals

Org Lett. 2007 May 24;9(11):2195-8. doi: 10.1021/ol070779i. Epub 2007 May 5.

Abstract

We describe how alkenes and alkynes can be hydrogenated under mild conditions by hydrogen transfer from water mediated by titanocene(III) and a substoichiometric quantity of one of the late transition metals usually employed as hydrogenation catalysts. This process proceeds presumably by H-atom transfer from TiIII-coordinated water to the late transition metal partner (depicted in the drawing above), a mechanism in support of which we provide theoretical and experimental evidence.