Characterization of a protein kinase B inhibitor in vitro and in insulin-treated liver cells

Diabetes. 2007 Sep;56(9):2218-27. doi: 10.2337/db07-0343. Epub 2007 Jun 11.

Abstract

Objective: Abnormal expression of the hepatic gluconeogenic genes (glucose-6-phosphatase [G6Pase] and PEPCK) contributes to hyperglycemia. These genes are repressed by insulin, but this process is defective in diabetic subjects. Protein kinase B (PKB) is implicated in this action of insulin. An inhibitor of PKB, Akt inhibitor (Akti)-1/2, was recently reported; however, the specificity and efficacy against insulin-induced PKB was not reported. Our aim was to characterize the specificity and efficacy of Akti-1/2 in cells exposed to insulin and then establish whether inhibition of PKB is sufficient to prevent regulation of hepatic gene expression by insulin.

Research design and methods: Akti-1/2 was assayed against 70 kinases in vitro and its ability to block PKB activation in cells exposed to insulin fully characterized.

Results: Akti-1/2 exhibits high selectivity toward PKBalpha and PKBbeta. Complete inhibition of PKB activity is achieved in liver cells incubated with 1-10 mumol/l Akti-1/2, and this blocks insulin regulation of PEPCK and G6Pase expression. Our data demonstrate that only 5-10% of maximal insulin-induced PKB is required to fully repress PEPCK and G6Pase expression. Finally, we demonstrate reduced insulin sensitivity of these gene promoters in cells exposed to submaximal concentrations of Akti-1/2; however, full repression of the genes can still be achieved by high concentrations of insulin.

Conclusions: This work establishes the requirement for PKB activity in the insulin regulation of PEPCK, G6Pase, and a third insulin-regulated gene, IGF-binding protein-1 (IGFBP1); suggests a high degree of functional reserve; and identifies Akti-1/2 as a useful tool to delineate PKB function in the liver.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Benzylamines / pharmacology
  • Carcinoma, Hepatocellular
  • Cell Line, Tumor
  • Enzyme Inhibitors / pharmacology*
  • Genes, Reporter
  • Gluconeogenesis / drug effects
  • Insulin / pharmacology*
  • Liver / drug effects
  • Liver / physiology*
  • Liver Neoplasms
  • Proto-Oncogene Proteins c-akt / antagonists & inhibitors
  • Proto-Oncogene Proteins c-akt / metabolism*
  • Quinoxalines / pharmacology
  • Rats
  • Reverse Transcriptase Polymerase Chain Reaction

Substances

  • Akt-I-1,2 compound
  • Benzylamines
  • Enzyme Inhibitors
  • Insulin
  • Quinoxalines
  • Proto-Oncogene Proteins c-akt