Polyfunctionalized pyrrolidines by Ugi multicomponent reaction followed by palladium-mediated SN2' cyclizations

J Org Chem. 2008 Feb 15;73(4):1608-11. doi: 10.1021/jo702087x. Epub 2008 Jan 15.

Abstract

A 4-component Ugi reaction with a suitable isocyanide, followed by a novel secondary transformation involving a Pd(II)-mediated (R5 = H) or a Pd(0)-mediated (R5 = CO2Me) SN2' cyclization to give highly functionalized N-acyl-2-vinylpyrrolidines, is reported. The overall yields are usually good and in most cases the Pd(0)-catalyzed reaction gave the final product in almost quantitative yield.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cyclization
  • Gas Chromatography-Mass Spectrometry
  • Magnetic Resonance Spectroscopy
  • Palladium / chemistry*
  • Pyrrolidines / chemistry*
  • Spectrophotometry, Infrared
  • Spectrophotometry, Ultraviolet

Substances

  • Pyrrolidines
  • Palladium