Biomimetic total synthesis of malbrancheamide and malbrancheamide B

J Org Chem. 2008 Apr 18;73(8):3116-9. doi: 10.1021/jo800116y. Epub 2008 Mar 18.

Abstract

The biomimetic total syntheses of both malbrancheamide and malbrancheamide B are reported. The synthesis of the two monochloro species enabled the structure of malbrancheamide B to be unambiguously assigned. The syntheses each feature an intramolecular Diels-Alder reaction of a 5-hydroxypyrazin-2(1H)-one to construct the bicyclo[2.2.2]diazaoctane core, which has also been proposed as the biosynthetic route to these compounds.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amides / chemistry
  • Biomimetics*
  • Heterocyclic Compounds, 4 or More Rings / chemical synthesis*
  • Heterocyclic Compounds, 4 or More Rings / chemistry
  • Indole Alkaloids
  • Molecular Structure
  • Oxidation-Reduction

Substances

  • Amides
  • Heterocyclic Compounds, 4 or More Rings
  • Indole Alkaloids
  • malbrancheamide