Crystallization and preliminary X-ray diffraction analysis of human IL-22 bound to the extracellular IL-22R1 chain

Acta Crystallogr Sect F Struct Biol Cryst Commun. 2008 Apr 1;64(Pt 4):266-9. doi: 10.1107/S1744309108004752. Epub 2008 Mar 21.

Abstract

Interleukin-22 (IL-22) is a potent mediator of cellular inflammatory responses. Crystals of IL-22 bound to the extracellular high-affinity cell-surface receptor sIL-22R1 have been grown from polyethylene glycol solutions. Crystals suitable for X-ray diffraction analysis were only obtained with mutants of IL-22 and sIL-22R1 that removed the N-linked glycosylation sites found in the wild-type amino-acid sequences. The crystals belonged to space group P2(1), with unit-cell parameters a = 50.43, b = 76.33, c = 114.92 A, beta = 92.45 degrees , and diffracted X-rays to 3.2 A resolution. The crystallographic asymmetric unit contained two IL-22-sIL-22R1 complexes, corresponding to a solvent content of approximately 52%.

Publication types

  • Comparative Study
  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Crystallization
  • Extracellular Space / chemistry
  • Extracellular Space / genetics
  • Extracellular Space / metabolism
  • Humans
  • Interleukin-22
  • Interleukins / chemistry*
  • Interleukins / genetics
  • Interleukins / metabolism*
  • Mutagenesis, Site-Directed
  • Protein Binding
  • Receptor Cross-Talk*
  • Receptors, Interleukin / chemistry*
  • Receptors, Interleukin / genetics
  • Receptors, Interleukin / metabolism*
  • X-Ray Diffraction

Substances

  • Interleukins
  • Receptors, Interleukin
  • interleukin-22 receptor