Crystal structure of the Ca(2+)-form and Ca(2+)-binding kinetics of metastasis-associated protein, S100A4

FEBS Lett. 2008 May 28;582(12):1651-6. doi: 10.1016/j.febslet.2008.04.017. Epub 2008 Apr 22.

Abstract

S100A4 takes part in control of tumour cell migration and contributes to metastatic spread in in vivo models. In the active dimeric Ca(2+)-bound state it interacts with multiple intracellular targets. Conversely, oligomeric forms of S100A4 are linked with the extracellular function of this protein. We report the 1.5A X-ray crystal structure of Ca(2+)-bound S100A4 and use it to identify the residues involved in target recognition and to derive a model of the oligomeric state. We applied stopped-flow analysis of tyrosine fluorescence to derive kinetics of S100A4 activation by Ca(2+) (k(on)=3.5 microM(-1)s(-1), k(off)=20s(-1)).

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Calcium / chemistry*
  • Crystallography, X-Ray
  • Fluorescence
  • Humans
  • Kinetics
  • Ligands
  • Molecular Sequence Data
  • Neoplasm Metastasis
  • Protein Binding
  • Protein Conformation
  • S100 Calcium-Binding Protein A4
  • S100 Proteins / chemistry*
  • Tyrosine / analysis

Substances

  • Ligands
  • S100 Calcium-Binding Protein A4
  • S100 Proteins
  • S100A4 protein, human
  • Tyrosine
  • Calcium