Purification and partial characterization of recombinant human differentiation-stimulating factor

Protein Expr Purif. 1990 Sep;1(1):54-62. doi: 10.1016/1046-5928(90)90046-2.

Abstract

Recombinant human differentiation-stimulating factor (rhD-factor) has been isolated to greater than 95% purity from Chinese hamster ovary cells. RhD-factor is a glycoprotein with an apparent molecular weight of 45.6 kDa as determined by sodium dodecyl sulfate-polyacrylamide gel electrophoresis. On gel filtration in 6 M guanidine-hydrochloride, rhD-factor elutes with an apparent molecular weight of 21.5 kDa; it elutes with an apparent molecular weight of 44.8 kDa under neutral pH (native) conditions. The amino-terminal sequence (12 residues) is consistent with the expected sequence derived from the genomic DNA sequence. Recombinant D-factor is heavily glycosylated with 30% by weight neutral sugar and 12% sialic acid. The ED50 for rhD-factor was 0.25 ng/ml. Trifluoromethanesulfonic acid-deglycosylated rhD-factor has a biological activity comparable to that of the native recombinant protein (ED50 = 0.40 ng/ml). The biological activity of rhD-factor was stable at pH 1 for 40 h, in 6 M guanidine-HCl containing buffers with or without reducing agent, and in 1% SDS. Carboxymethylation of D-factor after reduction totally destroyed biological activity.

MeSH terms

  • Amino Acid Sequence
  • Amino Acids / analysis
  • Animals
  • CHO Cells
  • Chromatography / methods
  • Cricetinae
  • Glycosylation
  • Growth Inhibitors / chemistry
  • Growth Inhibitors / isolation & purification*
  • Humans
  • Hydrogen-Ion Concentration
  • Interleukin-6*
  • Leukemia Inhibitory Factor
  • Lymphokines / chemistry
  • Lymphokines / isolation & purification*
  • Molecular Sequence Data
  • Molecular Weight
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / isolation & purification

Substances

  • Amino Acids
  • Growth Inhibitors
  • Interleukin-6
  • LIF protein, human
  • Leukemia Inhibitory Factor
  • Lymphokines
  • Recombinant Proteins