A model for the shuttle motions of puerarin and daidzin inside the cavity of β-cyclodextrin in aqueous acetic acid: insights from molecular dynamics simulations

J Mol Model. 2012 Jan;18(1):221-7. doi: 10.1007/s00894-011-1036-1. Epub 2011 Apr 27.

Abstract

Acetic acid acts as one component of the mobile phase to influence separation of puerarin from daidzin when using β-cyclodextrin-substituted media. In this work considering an explicit acetic acid solution, host-guest complexes of β-cyclodextrin (β-CD) with puerarin and daidzin were investigated by molecular dynamics simulations. Computational results indicate different shuttle motions of puerarin and daidzin inside the cavity of β-CD. A model detailing the shuttle motion was constructed, and the relationships between shuttle depth and guest rotation angles, hydrogen bonds, and host-guest interaction energies were analyzed. The results can be used to explain the chromatographic retention mechanisms of puerarin and daidzin with β-CD, and to explore the complexity of host-guest interactions involving β-CD.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acetic Acid / chemistry*
  • Chromatography / methods
  • Isoflavones / chemistry*
  • Models, Molecular
  • Molecular Dynamics Simulation
  • beta-Cyclodextrins / chemistry*

Substances

  • Isoflavones
  • beta-Cyclodextrins
  • daidzin
  • betadex
  • Acetic Acid
  • puerarin