Urine steroid metabolomics as a biomarker tool for detecting malignancy in adrenal tumors

J Clin Endocrinol Metab. 2011 Dec;96(12):3775-84. doi: 10.1210/jc.2011-1565. Epub 2011 Sep 14.

Abstract

Context: Adrenal tumors have a prevalence of around 2% in the general population. Adrenocortical carcinoma (ACC) is rare but accounts for 2-11% of incidentally discovered adrenal masses. Differentiating ACC from adrenocortical adenoma (ACA) represents a diagnostic challenge in patients with adrenal incidentalomas, with tumor size, imaging, and even histology all providing unsatisfactory predictive values.

Objective: Here we developed a novel steroid metabolomic approach, mass spectrometry-based steroid profiling followed by machine learning analysis, and examined its diagnostic value for the detection of adrenal malignancy.

Design: Quantification of 32 distinct adrenal derived steroids was carried out by gas chromatography/mass spectrometry in 24-h urine samples from 102 ACA patients (age range 19-84 yr) and 45 ACC patients (20-80 yr). Underlying diagnosis was ascertained by histology and metastasis in ACC and by clinical follow-up [median duration 52 (range 26-201) months] without evidence of metastasis in ACA. Steroid excretion data were subjected to generalized matrix learning vector quantization (GMLVQ) to identify the most discriminative steroids.

Results: Steroid profiling revealed a pattern of predominantly immature, early-stage steroidogenesis in ACC. GMLVQ analysis identified a subset of nine steroids that performed best in differentiating ACA from ACC. Receiver-operating characteristics analysis of GMLVQ results demonstrated sensitivity = specificity = 90% (area under the curve = 0.97) employing all 32 steroids and sensitivity = specificity = 88% (area under the curve = 0.96) when using only the nine most differentiating markers.

Conclusions: Urine steroid metabolomics is a novel, highly sensitive, and specific biomarker tool for discriminating benign from malignant adrenal tumors, with obvious promise for the diagnostic work-up of patients with adrenal incidentalomas.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adrenal Cortex Hormones / urine*
  • Adrenal Cortex Neoplasms / diagnosis*
  • Adrenal Cortex Neoplasms / pathology
  • Adrenal Cortex Neoplasms / urine
  • Adrenocortical Adenoma / diagnosis*
  • Adrenocortical Adenoma / pathology
  • Adrenocortical Adenoma / urine
  • Adrenocortical Carcinoma / diagnosis*
  • Adrenocortical Carcinoma / pathology
  • Adrenocortical Carcinoma / urine
  • Adult
  • Aged
  • Aged, 80 and over
  • Biomarkers / urine
  • Diagnosis, Differential
  • Female
  • Humans
  • Male
  • Mass Spectrometry
  • Metabolomics
  • Middle Aged

Substances

  • Adrenal Cortex Hormones
  • Biomarkers