In vitro and in vivo skin anti-aging evaluation of gel containing niosomes loaded with a semi-purified fraction containing gallic acid from Terminalia chebula galls

Pharm Biol. 2011 Nov;49(11):1190-203. doi: 10.3109/13880209.2011.576347.

Abstract

Context: The galls of Terminalia chebula Retz. (Combretaceae) frequently appear in many Thai Lanna medicinal plant recipes for promotion of longevity.

Objective: The objective of this study was to evaluate the skin anti-aging of gel containing niosomes loaded with a semi-purified fraction containing gallic acid from T. chebula galls.

Method: The semi-purified fraction containing phenolic compounds including gallic acid isolated from T. chebula galls loaded in non-elastic or elastic niosomes, and its developed gel, were evaluated for rabbit skin irritation by the closed patch test and skin anti-aging in human volunteers by measuring skin elasticity and roughness.

Results: Gel containing the fraction unloaded (SS) or loaded in non-elastic (SN) or elastic (SE) niosomes and gallic acid loaded in non-elastic (GN) or elastic (GE) niosomes showed no skin irritation, whereas the unloaded gallic acid (GS) gave the irritation in rabbit's skin by the closed patch test. The % parameter changes of skin elastic recovery and skin elastic extension when applied with SN and SE gels were +28.73 and +32.57; -21.25 and -22.63%, respectively. SN and SE gel also showed a significant decrease of the maximum and average roughness values with the parameter changes of -29.43 and -32.38; -39.47 and -35.28%, respectively.

Conclusion: The semi-purified fraction loaded in niosomes indicated not only higher chemical stability of gallic acid containing in the fraction, but also more in vivo anti-aging activities than the unloaded fraction when incorporated in gel.

Publication types

  • Controlled Clinical Trial
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Administration, Cutaneous
  • Adult
  • Animals
  • Biphenyl Compounds / chemistry
  • Cells, Cultured
  • Dermatologic Agents / administration & dosage
  • Dermatologic Agents / chemistry
  • Dermatologic Agents / isolation & purification
  • Dermatologic Agents / pharmacology*
  • Dermatologic Agents / toxicity
  • Dose-Response Relationship, Drug
  • Drug Stability
  • Elasticity
  • Female
  • Fibroblasts / drug effects
  • Fibroblasts / metabolism
  • Gallic Acid / administration & dosage
  • Gallic Acid / chemistry
  • Gallic Acid / isolation & purification
  • Gallic Acid / pharmacology*
  • Gallic Acid / toxicity
  • Gels
  • Humans
  • Liposomes
  • Male
  • Matrix Metalloproteinase 2 / metabolism
  • Matrix Metalloproteinase Inhibitors
  • Middle Aged
  • Picrates / chemistry
  • Plant Extracts / administration & dosage
  • Plant Extracts / chemistry
  • Plant Extracts / isolation & purification
  • Plant Extracts / pharmacology*
  • Plant Extracts / toxicity
  • Plant Tumors
  • Plants, Medicinal
  • Rabbits
  • Skin / drug effects*
  • Skin / metabolism
  • Skin / pathology
  • Skin Aging / drug effects*
  • Skin Irritancy Tests
  • Skin Pigmentation / drug effects
  • Terminalia* / chemistry
  • Thailand
  • Time Factors

Substances

  • Biphenyl Compounds
  • Dermatologic Agents
  • Gels
  • Liposomes
  • Matrix Metalloproteinase Inhibitors
  • Picrates
  • Plant Extracts
  • Gallic Acid
  • 1,1-diphenyl-2-picrylhydrazyl
  • MMP2 protein, human
  • Matrix Metalloproteinase 2