Solution NMR structure, backbone dynamics, and heme-binding properties of a novel cytochrome c maturation protein CcmE from Desulfovibrio vulgaris

Biochemistry. 2012 May 8;51(18):3705-7. doi: 10.1021/bi300457b. Epub 2012 Apr 24.

Abstract

Cytochrome c maturation protein E, CcmE, plays an integral role in the transfer of heme to apocytochrome c in many prokaryotes and some mitochondria. A novel subclass featuring a heme-binding cysteine has been identified in archaea and some bacteria. Here we describe the solution NMR structure, backbone dynamics, and heme binding properties of the soluble C-terminal domain of Desulfovibrio vulgaris CcmE, dvCcmE'. The structure adopts a conserved β-barrel OB fold followed by an unstructured C-terminal tail encompassing the CxxxY heme-binding motif. Heme binding analyses of wild-type and mutant dvCcmE' demonstrate the absolute requirement of residue C127 for noncovalent heme binding in vitro.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Outer Membrane Proteins / chemistry*
  • Bacterial Outer Membrane Proteins / metabolism
  • Cytochromes c / metabolism
  • Desulfovibrio vulgaris / chemistry
  • Heme / metabolism*
  • Hemeproteins / chemistry*
  • Hemeproteins / metabolism
  • Magnetic Resonance Spectroscopy
  • Protein Structure, Tertiary

Substances

  • Bacterial Outer Membrane Proteins
  • Hemeproteins
  • Heme
  • Cytochromes c