A novel approach to capillary plasma microsampling for quantitative bioanalysis

Bioanalysis. 2013 May;5(9):1131-5. doi: 10.4155/bio.13.58.

Abstract

Background: A novel device and procedure for the collection and isolation of microvolumes of plasma have been developed and two pilot rodent PK studies have been completed.

Results: This method involves collection of blood into a plastic-wrapped, EDTA-coated capillary tube, containing a small amount of a thixotropic gel and a porous plug. Following blood collection, the capillary is placed into a secondary labeled container suitable for centrifugation and plasma is generated. During centrifugation, the thixotropic gel isolates the plasma from the red blood cells and creates a physical barrier between the two matrices. The plasma is then dispensed from the capillary tube into a separate container for storage or processing.

Conclusion: A simple and robust novel approach for the collection of small plasma volumes from rodent TK studies has been demonstrated.

MeSH terms

  • Animals
  • Biological Assay / instrumentation
  • Biological Assay / methods*
  • Blood Specimen Collection / instrumentation
  • Blood Specimen Collection / methods*
  • Chromatography, High Pressure Liquid
  • Humans
  • Rats
  • Rats, Wistar
  • Tandem Mass Spectrometry