Characterization of estrogen response element binding proteins as biomarkers of breast cancer behavior

Clin Biochem. 2013 Nov;46(16-17):1739-46. doi: 10.1016/j.clinbiochem.2013.07.005. Epub 2013 Jul 16.

Abstract

Background: While investigating estrogen response element (ERE) binding properties of human estrogen receptor-α (hERα) in breast cancer cytosols, other ERE-binding proteins (ERE-BP) were observed.

Design and methods: Recognition properties of ERE-BP were evaluated by electrophoretic mobility shift assays (EMSA) with ERE sequences of the 5'-flanking region of the estrogen responsive gene vitellogenin A2 (VitA2). Cytosols were incubated 16 h, 4 °C with [32P]ERE sequences and separated by EMSA. A method of estimating ERE-BP levels was developed by measuring band intensity from EMSA profiles, expressed in digital light units (DLU)/μg protein and normalized to total DLU. ERE-BP were purified by affinity chromatography and EMSA, and then identified by mass spectrometry.

Results: ERE-BP in cytosols did not supershift in the presence of anti-hERα or anti-hERβ antibodies recognizing different ER epitopes suggesting that they are not fragments of either receptor isoform. ERE-BP competed with hERα for binding to VitA2-ERE. Increased levels of ERE-BP DNA-binding activities measured in 310 cytosols prepared from breast cancer biopsies correlated with decreased patient survival. Strikingly, breast cancer patients with ER negative status and high ERE-BP expression exhibited the poorest disease-free and overall survival. After purification, ERE-BP were identified as Ku70 (XRCC6) and Ku80 (XRCC5) using mass spectrometry. ERE-BP were confirmed to be Ku70/80 by supershift assay.

Conclusion: Presence of these novel ERE-binding proteins in a breast carcinoma is a strong predictor of poor prognosis. Our results suggest that ERE-BP, identified as Ku70/Ku80, in cytosols prepared from breast carcinoma biopsies are useful biomarkers for assessing risk of breast cancer recurrence.

Keywords: Biomarker; Breast cancer; Estrogen response element.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antibodies, Neoplasm / immunology
  • Antigens, Nuclear / metabolism
  • Binding, Competitive
  • Biomarkers, Tumor / metabolism*
  • Cytosol / metabolism
  • DNA, Neoplasm / metabolism
  • DNA-Binding Proteins / metabolism
  • Disease-Free Survival
  • Estrogen Receptor alpha / metabolism
  • Estrogen Receptor beta / metabolism
  • Estrogens / metabolism*
  • Female
  • Humans
  • Ku Autoantigen
  • Mass Spectrometry
  • Neoplasm Proteins / metabolism*
  • Protein Binding
  • Response Elements / genetics*
  • Tissue Extracts

Substances

  • Antibodies, Neoplasm
  • Antigens, Nuclear
  • Biomarkers, Tumor
  • DNA, Neoplasm
  • DNA-Binding Proteins
  • ESR1 protein, human
  • Estrogen Receptor alpha
  • Estrogen Receptor beta
  • Estrogens
  • Neoplasm Proteins
  • Tissue Extracts
  • Xrcc6 protein, human
  • Ku Autoantigen