Ocular penetration and pharmacokinetics of topical clarithromycin eye drops to rabbits

J Ocul Pharmacol Ther. 2014 Feb;30(1):42-8. doi: 10.1089/jop.2013.0042. Epub 2013 Nov 7.

Abstract

Purpose: To evaluate the ocular pharmacokinetics of clarithromycin (CLA) eye drops topically applied to the corneas of rabbits.

Methods: One 50-μL drop of CLA (0.25%) was administered to each New Zealand white rabbit in a single dose group, and one 50-μL drop of CLA was administered 6 times at 5-min intervals to each rabbit in a loading dose group. The effect of debridement on corneal penetration was also investigated in a de-epithelium group. The drug concentrations in the cornea and aqueous humor (AH) were assayed using high-performance liquid chromatography with tandem mass spectrometry (HPLC-MS/MS) analysis.

Results: Maximum CLA levels were achieved in the corneas and AH at 15 and 60 min, respectively, in the intact epithelium eyes in the single dose group (24.54±10.64 μg/g and 0.78±0.22 μg/mL, respectively, mean±the standard error of the mean, n=8). In the loading dose group, 30 min after the last application, the CLA level in the corneas reached 92.26±17.62 μg/g. In the loading dose group, the drug levels in the corneas and AH were significantly increased compared with the drug levels in the corneas with the intact epithelium and de-epithelium eyes in the single dose group at the corresponding time points (P<0.05). The estimated CLA half-lives in the corneas and AH for the intact eyes were 103.28 and 132.61 min, respectively.

Conclusion: Therapeutic CLA levels can be achieved in rabbit corneas after topically applying the drug with eye drops.

MeSH terms

  • Administration, Ophthalmic
  • Animals
  • Anti-Bacterial Agents / administration & dosage
  • Anti-Bacterial Agents / pharmacokinetics*
  • Aqueous Humor / metabolism*
  • Chromatography, High Pressure Liquid / methods
  • Clarithromycin / administration & dosage
  • Clarithromycin / pharmacokinetics*
  • Cornea / metabolism*
  • Epithelium, Corneal / metabolism
  • Female
  • Half-Life
  • Male
  • Ophthalmic Solutions
  • Rabbits
  • Tandem Mass Spectrometry / methods
  • Time Factors
  • Tissue Distribution

Substances

  • Anti-Bacterial Agents
  • Ophthalmic Solutions
  • Clarithromycin