Pd-catalyzed highly regio-, diastereo-, and enantioselective allylic alkylation of α-fluorophosphonates

Chem Commun (Camb). 2014 Jun 28;50(51):6751-3. doi: 10.1039/c4cc02158d.

Abstract

Highly efficient Pd-catalyzed asymmetric allylic alkylation reaction of ethyl-2-fluoro-2-(diethoxyphosphoryl)acetate with monosubstituted allylic substrates has been developed, affording corresponding α-fluorophosphonates with two chiral centers in high regio-, diastereo- and enantio-selectivities. The usefulness of the products in organic synthesis has been demonstrated.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkylation
  • Allyl Compounds / chemical synthesis*
  • Catalysis
  • Indicators and Reagents
  • Ligands
  • Organofluorophosphonates / chemistry*
  • Palladium / chemistry*
  • Stereoisomerism

Substances

  • Allyl Compounds
  • Indicators and Reagents
  • Ligands
  • Organofluorophosphonates
  • Palladium