Access to 4-alkylaminopyridazine derivatives via nitrogen-assisted regioselective Pd-catalyzed reactions

J Org Chem. 2014 Nov 7;79(21):10311-22. doi: 10.1021/jo501930s. Epub 2014 Oct 27.

Abstract

3-Substituted, 6-substituted, and unsymmetrical 3,6-disubstituted 4-alkylaminopyridazines were prepared from a sequence of three chemo- and regioselective reactions combining amination and palladium-catalyzed cross-coupling reactions, such as reductive dehalogenation and Suzuki-Miyaura reactions. Extension of the methodology to Sonogashira reaction yielded a novel class of 3-substituted pyrrolopyridazines.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amines / chemistry*
  • Catalysis
  • Molecular Structure
  • Nitrogen / chemistry*
  • Palladium / chemistry
  • Pyridazines / chemistry*
  • Pyrroles / chemistry*

Substances

  • Amines
  • Pyridazines
  • Pyrroles
  • Pyrrolopyridazine
  • Palladium
  • Nitrogen