Development and characterization of recombinant antibody fragments that recognize and neutralize in vitro Stx2 toxin from Shiga toxin-producing Escherichia coli

PLoS One. 2015 Mar 19;10(3):e0120481. doi: 10.1371/journal.pone.0120481. eCollection 2015.

Abstract

Background: Stx toxin is a member of the AB5 family of bacterial toxins: the active A subunit has N-glycosidase activity against 28S rRNA, resulting in inhibition of protein synthesis in eukaryotic cells, and the pentamer ligand B subunits (StxB) bind to globotria(tetra)osylceramide receptors (Gb3/Gb4) on the cell membrane. Shiga toxin-producing Escherichia coli strains (STEC) may produce Stx1 and/or Stx2 and variants. Strains carrying Stx2 are considered more virulent and related to the majority of outbreaks, besides being usually associated with hemolytic uremic syndrome in humans. The development of tools for the detection and/or neutralization of these toxins is a turning point for early diagnosis and therapeutics. Antibodies are an excellent paradigm for the design of high-affinity, protein-based binding reagents used for these purposes.

Methods and findings: In this work, we developed two recombinant antibodies; scFv fragments from mouse hybridomas and Fab fragments by phage display technology using a human synthetic antibody library. Both fragments showed high binding affinity to Stx2, and they were able to bind specifically to the GKIEFSKYNEDDTF region of the Stx2 B subunit and to neutralize in vitro the cytotoxicity of the toxin up to 80%. Furthermore, the scFv fragments showed 79% sensitivity and 100% specificity in detecting STEC strains by ELISA.

Conclusion: In this work, we developed and characterized two recombinant antibodies against Stx2, as promising tools to be used in diagnosis or therapeutic approaches against STEC, and for the first time, we showed a human monovalent molecule, produced in bacteria, able to neutralize the cytotoxicity of Stx2 in vitro.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Antibodies, Neutralizing / metabolism*
  • Cell Line
  • Humans
  • Hybridomas / immunology
  • Immunoglobulin Fab Fragments / metabolism*
  • Mice
  • Peptide Library
  • Sensitivity and Specificity
  • Shiga Toxin 2 / antagonists & inhibitors*
  • Shiga-Toxigenic Escherichia coli / immunology
  • Shiga-Toxigenic Escherichia coli / metabolism*
  • Single-Chain Antibodies / genetics
  • Single-Chain Antibodies / metabolism*

Substances

  • Antibodies, Neutralizing
  • Immunoglobulin Fab Fragments
  • Peptide Library
  • Shiga Toxin 2
  • Single-Chain Antibodies

Grants and funding

This research was supported by grants 11/12928-2 from São Paulo Research Foundation (FAPESP) and from Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq –301302/2013-8) to RMFP. DL (FAPESP – 10/20148-4 and 13/03160-9) and LBR were recipients of FAPESP fellowships. The funders had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript.