Phytoene Desaturase from Oryza sativa: Oligomeric Assembly, Membrane Association and Preliminary 3D-Analysis

PLoS One. 2015 Jul 6;10(7):e0131717. doi: 10.1371/journal.pone.0131717. eCollection 2015.

Abstract

Recombinant phytoene desaturase (PDS-His6) from rice was purified to near-homogeneity and shown to be enzymatically active in a biphasic, liposome-based assay system. The protein contains FAD as the sole protein-bound redox-cofactor. Benzoquinones, not replaceable by molecular oxygen, serve as a final electron acceptor defining PDS as a 15-cis-phytoene (donor):plastoquinone oxidoreductase. The herbicidal PDS-inhibitor norflurazon is capable of arresting the reaction by stabilizing the intermediary FAD(red), while an excess of the quinone acceptor relieves this blockage, indicating competition. The enzyme requires its homo-oligomeric association for activity. The sum of data collected through gel permeation chromatography, non-denaturing polyacrylamide electrophoresis, chemical cross-linking, mass spectrometry and electron microscopy techniques indicate that the high-order oligomers formed in solution are the basis for an active preparation. Of these, a tetramer consisting of dimers represents the active unit. This is corroborated by our preliminary X-ray structural analysis that also revealed similarities of the protein fold with the sequence-inhomologous bacterial phytoene desaturase CRTI and other oxidoreductases of the GR2-family of flavoproteins. This points to an evolutionary relatedness of CRTI and PDS yielding different carotene desaturation sequences based on homologous protein folds.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biopolymers / chemistry*
  • Cell Membrane / enzymology
  • Crystallography, X-Ray
  • Mass Spectrometry
  • Microscopy, Electron, Scanning
  • Native Polyacrylamide Gel Electrophoresis
  • Oryza / enzymology*
  • Oxidoreductases / chemistry*
  • Oxidoreductases / isolation & purification
  • Oxidoreductases / metabolism
  • Protein Binding
  • Protein Conformation

Substances

  • Biopolymers
  • Oxidoreductases
  • phytoene dehydrogenase

Grants and funding

This work was supported by the European Union Seventh Framework Programme (FP7) Contract 244348, by the HarvestPlus Research Consortium (PB) and by the Deutsche Forschungsgemeinschaft (grant EI-520/3 to OE). Research in the laboratory of BW was supported by the Deutsche Forschungsgemeinschaft and the Excellence Initiative of the German Federal and State Governments Grant EXC 294 BIOSS Centre for Biological Signalling Studies (EXC 294 to BW). [URLs: Harvest Plus, www.harvestplus.org; EC Framework, http://ec.europa.eu/research/fp7/index_en.cfm; Deutsche Forschungsgemeinschaft, http://www.dfg.de/; Excellence initiative, http://www.dfg.de/en/research_funding/programmes/excellence_initiative/index.html]. The funders had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript.