1020MHz single-channel proton fast magic angle spinning solid-state NMR spectroscopy

J Magn Reson. 2015 Dec:261:1-5. doi: 10.1016/j.jmr.2015.10.003. Epub 2015 Oct 17.

Abstract

This study reports a first successful demonstration of a single channel proton 3D and 2D high-throughput ultrafast magic angle spinning (MAS) solid-state NMR techniques in an ultra-high magnetic field (1020MHz) NMR spectrometer comprised of HTS/LTS magnet. High spectral resolution is well demonstrated.

Keywords: Proton detection; Solid-state NMR; Structure elucidation; Ultra-high field; Ultrafast MAS.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Electromagnetic Fields
  • Histidine / chemistry
  • Magnetic Resonance Spectroscopy / methods*
  • Nuclear Magnetic Resonance, Biomolecular / methods
  • Protons*
  • Tyrosine / chemistry

Substances

  • Protons
  • Tyrosine
  • Histidine