Design and Modular Construction of a Polymeric Nanoparticle for Targeted Atherosclerosis Positron Emission Tomography Imaging: A Story of 25% (64)Cu-CANF-Comb

Pharm Res. 2016 Oct;33(10):2400-10. doi: 10.1007/s11095-016-1963-8. Epub 2016 Jun 10.

Abstract

Purpose: To assess the physicochemical properties, pharmacokinetic profiles, and in vivo positron emission tomography (PET) imaging of natriuretic peptide clearance receptors (NPRC) expressed on atherosclerotic plaque of a series of targeted, polymeric nanoparticles.

Methods: To control their structure, non-targeted and targeted polymeric (comb) nanoparticles, conjugated with various amounts of c-atrial natriuretic peptide (CANF, 0, 5, 10 and 25%), were synthesized by controlled and modular chemistry. In vivo pharmacokinetic evaluation of these nanoparticles was performed in wildtype (WT) C57BL/6 mice after (64)Cu radiolabeling. PET imaging was performed on an apolipoprotein E-deficient (ApoE(-/-)) mouse atherosclerosis model to assess the NPRC targeting efficiency. For comparison, an in vivo blood metabolism study was carried out in WT mice.

Results: All three (64)Cu-CANF-comb nanoparticles showed improved biodistribution profiles, including significantly reduced accumulation in both liver and spleen, compared to the non-targeted (64)Cu-comb. Of the three nanoparticles, the 25% (64)Cu-CANF-comb demonstrated the best NPRC targeting specificity and sensitivity in ApoE(-/-) mice. Metabolism studies showed that the radiolabeled CANF-comb was stable in blood up to 9 days. Histopathological analyses confirmed the up-regulation of NPRC along the progression of atherosclerosis.

Conclusion: The 25% (64)Cu-CANF-comb demonstrated its potential as a PET imaging agent to detect atherosclerosis progression and status.

Keywords: atherosclerosis; nanoparticle; natriuretic peptide clearance receptor; polymer synthesis; positron emission tomography.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Animals
  • Atherosclerosis / diagnostic imaging
  • Atherosclerosis / metabolism*
  • Atrial Natriuretic Factor / administration & dosage
  • Atrial Natriuretic Factor / chemistry
  • Atrial Natriuretic Factor / metabolism*
  • Copper Radioisotopes / administration & dosage
  • Copper Radioisotopes / chemistry
  • Copper Radioisotopes / metabolism*
  • Drug Delivery Systems / methods
  • Male
  • Mice
  • Mice, Inbred C57BL
  • Mice, Knockout
  • Nanoparticles / administration & dosage
  • Nanoparticles / chemistry
  • Nanoparticles / metabolism*
  • Polymers / administration & dosage
  • Polymers / chemistry
  • Polymers / metabolism*
  • Positron-Emission Tomography / methods*
  • Tissue Distribution / drug effects
  • Tissue Distribution / physiology

Substances

  • Copper Radioisotopes
  • Polymers
  • Atrial Natriuretic Factor