In vivo pharmacological evaluation and efficacy study of methotrexate-encapsulated polymer-coated layered double hydroxide nanoparticles for possible application in the treatment of osteosarcoma

Drug Deliv Transl Res. 2017 Apr;7(2):259-275. doi: 10.1007/s13346-016-0351-6.

Abstract

Considering the existing drawbacks of methotrexate (MTX) with respect to its solubility and toxicity, we incorporated it in a nanoceramic matrix, Mg-Al-layered double hydroxide (LDH) to form LDH-MTX nanoparticles, and the same was in turn encapsulated in a nontoxic and biodegradable polymer, poly (D,L-lactide-co-glycolide) (PLGA), to arrest the initial burst release and dose-dumping-related toxicity, already reported by our group. Our present study was designed to evaluate the pharmacokinetics, tissue distribution, survival rate of the test animals, and antitumor efficacy of the PLGA-LDH-MTX nanoparticles and its counterpart without LDH, PLGA-MTX nanoparticles compared with bare MTX. The median lethal dose (LD50) of the former was higher, compared with bare MTX, using Balb/c nude mice, indicating it to be completely safe for use. Also, a comparative pharmacokinetic and antitumour efficacy study using MTX, PLGA-MTX, and PLGA-LDH-MTX nanoparticles in osteosarcoma-induced Balb/c nude mice in vivo demonstrated superiority of PLGA-LDH-MTX as compared to PLGA-MTX and bare MTX. The results suggest that PLGA-LDH-MTX nanoparticles might exhibit potential advantages over the present-day chemotherapy over bare MTX, for the possibility of treatment of osteosarcoma.

Keywords: Antitumor efficacy; Hepatotoxicity and nephrotoxicity; Methotrexate; Mg–Al-layered double hydroxide; Pharmacokinetics; Poly(D,L-lactide-co-glycolide); Survival rate; Tissue distribution.

MeSH terms

  • Aluminum / metabolism
  • Animals
  • Antimetabolites, Antineoplastic / administration & dosage*
  • Antimetabolites, Antineoplastic / chemistry
  • Antimetabolites, Antineoplastic / pharmacokinetics
  • Antimetabolites, Antineoplastic / therapeutic use
  • Bone Neoplasms / drug therapy*
  • Bone Neoplasms / metabolism
  • Bone Neoplasms / pathology
  • Cell Line, Tumor
  • Female
  • Humans
  • Hydroxides / administration & dosage*
  • Hydroxides / chemistry
  • Hydroxides / pharmacokinetics
  • Hydroxides / therapeutic use
  • Kidney / drug effects
  • Lactic Acid / administration & dosage
  • Lactic Acid / chemistry
  • Lactic Acid / pharmacokinetics
  • Lactic Acid / therapeutic use
  • Liver / drug effects
  • Magnesium / metabolism
  • Male
  • Methotrexate / administration & dosage*
  • Methotrexate / chemistry
  • Methotrexate / pharmacokinetics
  • Methotrexate / therapeutic use
  • Mice, Inbred BALB C
  • Mice, Nude
  • Nanoparticles / administration & dosage*
  • Nanoparticles / chemistry
  • Nanoparticles / therapeutic use
  • Osteosarcoma / drug therapy*
  • Osteosarcoma / metabolism
  • Osteosarcoma / pathology
  • Polyglycolic Acid / administration & dosage
  • Polyglycolic Acid / chemistry
  • Polyglycolic Acid / pharmacokinetics
  • Polyglycolic Acid / therapeutic use
  • Polylactic Acid-Polyglycolic Acid Copolymer
  • Tumor Burden / drug effects

Substances

  • Antimetabolites, Antineoplastic
  • Hydroxides
  • Polylactic Acid-Polyglycolic Acid Copolymer
  • Polyglycolic Acid
  • Lactic Acid
  • Aluminum
  • Magnesium
  • Methotrexate