Acetone promoted 1,4-migration of an alkoxycarbonyl group on a syn-1,2-diamine

Tetrahedron Lett. 2017 Feb 15;58(7):597-601. doi: 10.1016/j.tetlet.2016.12.047. Epub 2017 Jan 3.

Abstract

A 2-protected cis-amino mitosene undergoes an irreversible acetone promoted isomerization and converts to the 1-isomer. Kinetic studies and DFT calculations of the reaction are reported. An organocatalytic mechanism is proposed, involving a covalent intermediate formed by reaction of the mitosene and acetone.

Keywords: Acetone; Alkoxycarbonyl migration; Mitosene; Organocatalytic mechanism.