NMR resonance assignments of RNase P protein from Thermotoga maritima

Biomol NMR Assign. 2018 Apr;12(1):183-187. doi: 10.1007/s12104-018-9806-7. Epub 2018 Feb 15.

Abstract

Ribonuclase P (RNase P) is an essential metallo-endonuclease that catalyzes 5' precursor-tRNA (ptRNA) processing and exists as an RNA-based enzyme in bacteria, archaea, and eukaryotes. In bacteria, a large catalytic RNA and a small protein component assemble to recognize and accurately cleave ptRNA and tRNA-like molecular scaffolds. Substrate recognition of ptRNA by bacterial RNase P requires RNA-RNA shape complementarity, intermolecular base pairing, and a dynamic protein-ptRNA binding interface. To gain insight into the binding specificity and dynamics of the bacterial protein-ptRNA interface, we report the backbone and side chain 1H, 13C, and 15N resonance assignments of the hyperthermophilic Thermatoga maritima RNase P protein in solution at 318 K. Our data confirm the formation of a stable RNA recognition motif (RRM) with intrinsic heterogeneity at both the N- and C-terminus of the protein, consistent with available structural information. Comprehensive resonance assignments of the bacterial RNase P protein serve as an important first step in understanding how coupled RNA binding and protein-RNA conformational changes give rise to ribonucleoprotein function.

Keywords: NMR resonance assignment; Protein–tRNA binding; RNase P; Ribonucleoprotein; TALOS-N prediction; Thermatoga maritima.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Nuclear Magnetic Resonance, Biomolecular*
  • Ribonuclease P / chemistry*
  • Thermotoga maritima / enzymology*

Substances

  • Ribonuclease P