Synthesis, activity, and docking studies of eugenol-based glucosides as new agents against Candida sp

Chem Biol Drug Des. 2018 Aug;92(2):1514-1524. doi: 10.1111/cbdd.13318. Epub 2018 May 18.

Abstract

Seventeen new synthetic derivatives of eugenol (6, 8-15 and 8'-15') were planned following literature reports on antifungal activities of nitroeugenol and eugenol glucoside. The anti-Candida activity of these compounds was investigated by in vitro assay, and the cytotoxicity evaluation was performed with the most active compounds. The peracetylated glucosides presented better biological results than their hydroxylated analogues. The glucoside 11, a 4-nitrobenzamide, showed the best potency (MIC50 range 11.0-151.84 μm), the wider spectrum of action, and overall the best selectivity indexes, especially against C. tropicalis (~30) and C. krusei (~15). To investigate its possible mechanism of action, glucoside 11 was subjected to molecular docking studies with Candida sp. enzymes involved in ergosterol biosynthesis. Results have shown that the peracetyl glucosyl moiety and the 4-nitrobenzamide group in 11 are effectively involved in its high affinity with the active site of squalene epoxidase.

Keywords: Candida spp.; antifungals; eugenol; glucosides; molecular docking.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antifungal Agents / chemical synthesis*
  • Antifungal Agents / pharmacology
  • Binding Sites
  • Candida / drug effects
  • Catalytic Domain
  • Eugenol / analogs & derivatives*
  • Fungal Proteins / antagonists & inhibitors
  • Fungal Proteins / metabolism
  • Glucosides / chemistry*
  • Glucosides / pharmacology
  • Microbial Sensitivity Tests
  • Molecular Docking Simulation
  • Squalene Monooxygenase / antagonists & inhibitors
  • Squalene Monooxygenase / metabolism
  • Structure-Activity Relationship
  • Thermodynamics

Substances

  • Antifungal Agents
  • Fungal Proteins
  • Glucosides
  • Eugenol
  • Squalene Monooxygenase