Hydrophobic Metal Halide Perovskites for Visible-Light Photoredox C-C Bond Cleavage and Dehydrogenation Catalysis

Angew Chem Int Ed Engl. 2019 Mar 11;58(11):3456-3460. doi: 10.1002/anie.201812225. Epub 2019 Feb 4.

Abstract

Two-dimensional lead and tin halide perovskites were prepared by intercalating the long alkyl group 1-hexadecylammonium (HDA) between the inorganic layers. We observed visible-light absorption, narrow-band photoluminescence, and nanosecond photoexcited lifetimes in these perovskites. Owing to their hydrophobicity and stability even in humid air, we applied these perovskites in the decarboxylation and dehydrogenation of indoline-2-carboxylic acids. (HDA)2 PbI4 or (HDA)2 SnI4 were investigated as photoredox catalysts for these reactions, and quantitative conversion and high yields were observed with the former.

Keywords: decarboxylation; hydrophobic perovskites; photocatalysis; photooxidation; two-dimensional materials.