Electrical Conductivity-Relay between Organic Charge-Transfer and Radical Salts toward Conductive Additive-Free Rechargeable Battery

ACS Appl Mater Interfaces. 2020 Jun 10;12(23):25748-25755. doi: 10.1021/acsami.0c03642. Epub 2020 May 29.

Abstract

In recent years, organic electrode materials have been strongly considered for use in sustainable batteries. However, most organic electrode materials have low electrical conductivity and require a lot of conductive additives, which decrease the effective capacity based on the entire electrode weight/volume. In this study, we propose a novel electrical conductivity-relay system that imparts electrical conductivity to organic small molecular electrodes without any conductive additive throughout the charge/discharge cycles. It consists of the combination of the charge-transfer phenomenon in a pristine state and the formation of organic radical salts in redox states. Herein, we demonstrate this electrical conductivity-relay system using a simply mixed molecular crystal couple of tetrathiafulvalene (TTF) and tetracyanoquinodimethane (TCNQ) as a cathode without any conductive additive and aqueous sodium bromide as an electrolyte. During charge/discharge, the electrical conductivity of the cathode is supported by charge-transfer at the TTF/TCNQ interface and (TTF)Brn (0.7 ≤ n ≤ 0.8) and NaTCNQ radical salts, and the cathode exhibits a specific capacity of 112 mAh g-1 and a retention rate of 80.7% at the 30th cycle. Furthermore, the molecular crystal couple electrode of TTF and TCNQ shows better charge/discharge performance than the pure charge-transfer complex electrode, indicating that this system expands candidates for organic electrode materials to various pairs and mixing ratios of small molecules that do not form charge-transfer complexes.

Keywords: charge-transfer; conductive additive-free cathode; organic battery; radical salt.