Determination of l-theanine in tea water using fluorescence-visualized paper-based sensors based on CdTe quantum dots/corn carbon dots and nano-porphyrin with chemometrics

J Sci Food Agric. 2021 Apr;101(6):2552-2560. doi: 10.1002/jsfa.10882. Epub 2020 Oct 31.

Abstract

Background: The quality of tea is influenced by numerous factors, especially l-theanine, which is one of the important markers used to evaluate the sweetness and freshness of tea. Sensitive, rapid, and accurate detection of l-theanine is therefore useful to identify the grade and quality of tea.

Results: A high-sensitivity, paper-based fluorescent sensor combined with chemometrics was established to detect l-theanine in tea water based on CdTe quantum dots / corn carbon dots and nano tetra pyridel-porphine zinc (ZnTPyP). To verify the reliability of this method, fluorescence spectra and fluorescence-visualized paper-based sensors were compared. The fluorescence spectrum method demonstrated a linear range of 1 to 10 000 nmol L-1 and a limit of detection (LOD) of 0.19 nmol L-1 . In the fluorescence-visualized paper-based sensors there was a linear range of 10-1000 nmol L-1 , and the LOD was 10 nmol L-1 . Partial least squares discriminant analysis (PLSDA) and partial least squares regression analysis (PLSR) were used successfully to determine l-theanine accurately in tea water with this approach. The accuracy of the PLSDA model was 100% both in the training set and the predicting set, and the correlation coefficient between the actual concentration and the predicted concentration was greater than 0.9997 in the PLSR model.

Conclusion: This fluorescence-visualized paper-based sensor, combined with chemometrics, could be applied efficiently to the practical analysis of tea water samples, which provides a new idea to ensure the flavor and quality of tea. © 2020 Society of Chemical Industry.

Keywords: l-theanine; CdTe quantum dots; chemometrics; corn carbon dots; fluorescence paper-based sensors; nano ZnTPyP.

Publication types

  • Evaluation Study

MeSH terms

  • Cadmium Compounds / chemistry
  • Fluorescence
  • Food Analysis / instrumentation
  • Food Analysis / methods*
  • Food Quality
  • Limit of Detection
  • Luminescent Measurements / instrumentation
  • Luminescent Measurements / methods*
  • Porphyrins / chemistry
  • Quantum Dots / chemistry
  • Tea / chemistry*
  • Tellurium / analysis*
  • Tellurium / chemistry
  • Zea mays / chemistry

Substances

  • Cadmium Compounds
  • Porphyrins
  • Tea
  • Tellurium
  • cadmium telluride