Evaluation of Physicochemical Properties Following Syringe-to-Syringe Mixing of Hyaluronic Acid Dermal Fillers

Dermatol Surg. 2020 Dec;46(12):1606-1612. doi: 10.1097/DSS.0000000000002806.

Abstract

Background: Historically, soft-tissue hyaluronic acid (HA) fillers have been mixed with agents to reduce pain or alter physicochemical properties.

Objective: Evaluate the impact of dilution and mixing on HA filler physicochemical properties.

Materials and methods: Crosslinked HA filler (VYC-20L, 20 mg/mL) was diluted to 15 mg/mL using saline through 5 or 10 passes between 2 syringes connected using a luer connector. Extrusion force, rheological properties, and microscopic appearance were assessed. Undiluted VYC-15L (15 mg/mL) served as the control.

Results: Average extrusion force was higher for diluted VYC-20L versus the control, with an increase in slope for gel diluted using 5 passes (0.65) and 10 passes (0.52) versus the control (<0.1). For diluted samples mixed with 5 or 10 passes, the rheological profile was different between the 2 halves of the syringe, with the second half more elastic than the first half, compared with the consistent profile of undiluted samples. Microscopically, diluted VYC-20L samples seemed more liquid near the luer and more particulate near the piston compared with the control, which was smooth throughout.

Conclusion: In addition to potentially introducing contamination, diluting or mixing soft-tissue HA fillers yields a heterogeneous product with physicochemical characteristics that vary substantially throughout the syringe.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Anesthetics, Local / administration & dosage
  • Anesthetics, Local / chemistry
  • Cosmetic Techniques
  • Dermal Fillers / administration & dosage
  • Dermal Fillers / chemistry*
  • Dermal Fillers / standards
  • Drug Combinations
  • Drug Compounding / instrumentation
  • Drug Compounding / methods*
  • Drug Compounding / standards
  • Drug Contamination / prevention & control
  • Hyaluronic Acid / administration & dosage
  • Hyaluronic Acid / chemistry*
  • Hyaluronic Acid / standards
  • Lidocaine / administration & dosage
  • Lidocaine / chemistry
  • Rheology
  • Saline Solution / chemistry
  • Syringes

Substances

  • Anesthetics, Local
  • Dermal Fillers
  • Drug Combinations
  • Saline Solution
  • Hyaluronic Acid
  • Lidocaine