Biophysical characterization of the CXC chemokine receptor 2 ligands

PLoS One. 2024 Apr 16;19(4):e0298418. doi: 10.1371/journal.pone.0298418. eCollection 2024.

Abstract

The chemokines of the immune system act as first responders by operating as chemoattractants, directing immune cells to specific locations of inflamed tissues. This promiscuous network is comprised of 50 ligands and 18 receptors where the ligands may interact with the receptors in various oligomeric states i.e., monomers, homodimers, and heterodimers. Chemokine receptors are G-protein coupled receptors (GPCRs) present in the membrane of immune cells. The migration of immune cells occurs in response to a concentration gradient of the ligands. Chemotaxis of neutrophils is directed by CXC-ligand (CXCL) activation of the membrane bound CXC chemokine receptor 2 (CXCR2). CXCR2 plays an important role in human health and is linked to disorders such as autoimmune disorders, inflammation, and cancer. Yet, despite their important role, little is known about the biophysical characteristics controlling ligand:ligand and ligand:receptor interaction essential for biological activity. In this work, we study the homodimers of three of the CXCR2 cognate ligands, CXCL1, CXCL5, and CXCL8. The ligands share high structural integrity but a low sequence identity. We show that the sequence diversity has evolved different binding affinities and stabilities for the CXC-ligands resulting in diverse agonist/antagonist behavior. Furthermore, CXC-ligands fold through a three-state mechanism, populating a folded monomeric state before associating into an active dimer.

MeSH terms

  • Chemokine CXCL1
  • Chemokines / metabolism
  • Chemotactic Factors / metabolism
  • Chemotaxis
  • Humans
  • Interleukin-8* / metabolism
  • Ligands
  • Receptors, Interleukin-8B* / genetics

Substances

  • Receptors, Interleukin-8B
  • Ligands
  • Interleukin-8
  • Chemokines
  • Chemokine CXCL1
  • Chemotactic Factors

Grants and funding

National Science Foundation (NSF) award number CHE2145906 the Hawaii Community Foundation (HCF) award number HCF40846 (013357-00002) The funders had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript.