Development and characterisation of orally disintegrating flurbiprofen tablets using SeDeM-ODT tool

PLoS One. 2024 Oct 29;19(10):e0309894. doi: 10.1371/journal.pone.0309894. eCollection 2024.

Abstract

In this study, SeDeM-ODT parametric tests were performed to determine the use of ludipress as a directly compressible tableting excipient for the development of a flurbiprofen orally disintegrating tablet. The preformulation features of different formulations (F1 -F9) were analyzed by the SeDeM-ODT tool which showed that all the powder blends were appropriate for direct compression since all the blends had index of good compressibility and bucodispersibility (IGCB) values above 5, signifying direct compression is the most appropriate method. The powder blend of the optimized formulation was assessed by the DSC-TGA technique. The optimization of nine different formulations blends of orally disintegrating tablets (ODTs) was prepared in various ratios by the implementation of design of experiments (DoE), using the central composite design by selecting ludipress (X1) (49-55%) and croscarmellose sodium (X2) (1-5%) while hardness, friability, and disintegration tests were selected as responses. The optimized formulations were evaluated by various tests and the results indicated that all the formulations were found to be in adequate range. Formulations were subjected to stability studies at accelerated states following ICH guidelines. Shelf life was found to be 51.144-56.186 months. Results of multiple-point dissolution studies revealed that formulations followed the Higuchi kinetic model. This study revealed that the SeDeM-ODT tool has been successfully used to determine the compression behavior of active compounds and their powder blends for the direct compression (DC) method in formulating flurbiprofen-ODT tablets.

MeSH terms

  • Administration, Oral
  • Anti-Inflammatory Agents, Non-Steroidal / administration & dosage
  • Anti-Inflammatory Agents, Non-Steroidal / chemistry
  • Chemistry, Pharmaceutical / methods
  • Drug Compounding / methods
  • Excipients / chemistry
  • Flurbiprofen* / administration & dosage
  • Flurbiprofen* / chemistry
  • Hardness
  • Powders
  • Solubility
  • Tablets* / chemistry

Substances

  • Flurbiprofen
  • Tablets
  • Powders
  • Excipients
  • Anti-Inflammatory Agents, Non-Steroidal

Grants and funding

The author(s) received no specific funding for this work.