Cycloaddition of Butadiene with Perfluoroethylene: Prediction of a Periselectivity Switch under Pressure

J Org Chem. 2024 Dec 6;89(23):17768-17772. doi: 10.1021/acs.joc.4c01361. Epub 2024 Nov 11.

Abstract

Defying the common Diels-Alder reactivity, the thermal cycloaddition between butadiene and tetrafluoroethylene (TFE) yields exclusively a [2 + 2] cycloadduct via a stepwise diradical mechanism. Here, we study the possibility of reverting to the normal [4 + 2] reactivity in this reaction under high pressure. DFT calculations using the eXtreme Pressure Polarizable Continuum Model (XP-PCM) suggest a more negative activation volume for the concerted [4 + 2] mechanism than the stepwise [2 + 2] mechanism and predict a switch in periselectivity at 1.4 gigapascal (GPa).