A versatile gold leaf immunosensor with a novel surface functionalization strategy based on protein L and trastuzumab for HER2 detection

Sci Rep. 2025 Jan 2;15(1):34. doi: 10.1038/s41598-024-83961-9.

Abstract

Although various sensors specifically developed for target analytes are available, affordable biosensing solutions with broad applicability are limited. In this study, a cost-effective biosensor for detecting human epidermal growth factor receptor 2 (HER2) was developed using custom-made gold leaf electrodes (GLEs). A novel strategy for antibody immobilization on a gold surface, for the first time mediated by protein L and HER2-specific antibody trastuzumab, was examined using commercial screen-printed gold electrodes and GLEs. A self-assembled monolayer of 11-mercaptoundecanoic acid (MUA) was formed on the gold surface, which was used to covalently immobilize protein L. Further binding of trastuzumab to the protein L was employed and HER2 detection was achieved through electrochemical impedance spectroscopy (EIS). The HER2 detection was examined in phosphate-buffered saline (PBS) and supplemented cell culture medium. The modified GLEs showed good specificity and high sensitivity of HER2 detection without any enrichment steps, achieving a limit of detection (LOD) of 1 ng mL- 1 in PBS and 2.7 ng mL- 1 in cell culture medium, making the proposed immunosensor a cost-effective and sensitive solution for detection in complex biological matrices.

Keywords: Cancer biomarker detection; Electrochemical immunosensor; Gold leaf electrodes; HER2 biosensor; Protein L; Trastuzumab.

MeSH terms

  • Antibodies, Immobilized / chemistry
  • Antibodies, Immobilized / immunology
  • Biosensing Techniques* / methods
  • Dielectric Spectroscopy / methods
  • Electrodes
  • Fatty Acids
  • Gold* / chemistry
  • Humans
  • Immunoassay / methods
  • Limit of Detection
  • Receptor, ErbB-2* / metabolism
  • Sulfhydryl Compounds
  • Trastuzumab*

Substances

  • Trastuzumab
  • Receptor, ErbB-2
  • Gold
  • ERBB2 protein, human
  • Antibodies, Immobilized
  • 11-mercaptoundecanoic acid
  • Fatty Acids
  • Sulfhydryl Compounds