Two adjacent N-terminal glutamines of BM-40 (osteonectin, SPARC) act as amine acceptor sites in transglutaminaseC-catalyzed modification

J Biol Chem. 1995 Oct 6;270(40):23415-20. doi: 10.1074/jbc.270.40.23415.

Abstract

The extracellular matrix protein BM-40 (osteonectin, SPARC) has recently been shown to be a major target for transglutaminase-catalyzed cross-linking in differentiating cartilage. In the present study we demonstrate that recombinant human BM-40 can be modified with [3H]putrescine in a 1:1 molar ratio by transglutaminaseC (tissue transglutaminase). Residues Gln3 and Gln4 were identified as major amine acceptor sites. This was confirmed with several mutant proteins, including deletions in the N-terminal domain I of BM-40, site-directed mutagenesis of the reactive glutamines, and fusion of the seven-amino acid-long N-terminal sequence (APQQEAL) to an unrelated protein. The results showed that the N-terminal target site is sufficient for modification by transglutaminase but at a low level. For high efficiency amine incorporation an intact domain I is required. The conservation of at least one of the transglutaminase target glutamines in the known vertebrate BM-40 sequences and their absence in an invertebrate homologue point to an important, but yet unknown, role of this modification in vertebrates.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Base Sequence
  • Binding Sites
  • Cross-Linking Reagents
  • DNA Primers / genetics
  • Drug Design
  • Glutamine / chemistry
  • Glutamine / genetics
  • Glutamine / metabolism
  • Guinea Pigs
  • Humans
  • Molecular Sequence Data
  • Molecular Structure
  • Mutagenesis, Site-Directed
  • Osteonectin / chemistry
  • Osteonectin / genetics
  • Osteonectin / metabolism*
  • Putrescine
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / genetics
  • Recombinant Proteins / metabolism
  • Substrate Specificity
  • Transglutaminases / metabolism*

Substances

  • Cross-Linking Reagents
  • DNA Primers
  • Osteonectin
  • Recombinant Proteins
  • Glutamine
  • Transglutaminases
  • Putrescine