Reversal of doxorubicin resistance and catalytic neutralization of lysosomes by a lipophilic imidazole

Biochim Biophys Acta. 1994 Apr 20;1191(1):103-8. doi: 10.1016/0005-2736(94)90237-2.

Abstract

A number of lipophilic nitrogenous bases, designed to act as membrane-active, catalytic proton transfer agents, were tested for their ability to neutralize the acidity of lysosomes, a model for other acidic intracellular vesicles involved in drug sorting. The most successful of these, an imidazole 1, caused a 1.7 unit rise in lysosomal pH of RAW cells at 100 microM, compared to a 0.2 and 1.4 unit rise for ammonium chloride at 100 microM and 10 mM, respectively. Compound 1 also exhibited potent reversal of doxorubicin (DOX) resistance in the HCT116-VM46 cell line by a factor of 14 over the sensitive strain, and superior to that of widely used verapamil (VRP) by a factor of 1.75 at 20 microM. It also has antiviral properties, and potential applications in other lysosome-related areas such as immunotoxin potentiation and the control of bacterial toxins, immune response, prion replication, malaria and intralysosomal microorganisms.

MeSH terms

  • Catalysis
  • Cells, Cultured
  • Doxorubicin / metabolism
  • Doxorubicin / pharmacology*
  • Drug Resistance
  • Humans
  • Hydrogen-Ion Concentration
  • Imidazoles / pharmacology*
  • Lysosomes / chemistry
  • Lysosomes / drug effects*
  • Tumor Cells, Cultured
  • Verapamil / pharmacology

Substances

  • Imidazoles
  • Doxorubicin
  • Verapamil