Extending crystallographic information with semiempirical quantum mechanics and molecular mechanics: a case of aspartic proteinases

J Chem Inf Comput Sci. 1993 Mar-Apr;33(2):270-4. doi: 10.1021/ci00012a014.

Abstract

The results of crystallographic analysis of a complex between an aspartic proteinase, endothiapepsin, and an inhibitor have been extended through the assignment of protons in the active site, to study various steps in the reaction with a substrate. Mechanistic implications are suggested as a consequence of semiempirical quantum mechanical calculations, indicating that most of the activation energy is required to bring the substrate from an initial binding mode to close distance to a water molecule.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Aspartic Acid Endopeptidases / antagonists & inhibitors
  • Aspartic Acid Endopeptidases / chemistry*
  • Binding Sites
  • HIV Protease / chemistry
  • HIV-1 / enzymology
  • Hydrogen Bonding
  • Molecular Sequence Data
  • Molecular Structure
  • Protons
  • Quantum Theory
  • Thermodynamics
  • X-Ray Diffraction*

Substances

  • Protons
  • Aspartic Acid Endopeptidases
  • Endothia aspartic proteinase
  • HIV Protease