Solid-phase competitive luminescence immunoassay for lysozyme in faeces

Clin Chim Acta. 1995 Aug 14;239(2):167-77. doi: 10.1016/0009-8981(95)06112-q.

Abstract

We have developed a new simple solid-phase luminescence immunoassay (LIA) for the determination of faecal lysozyme. The assay utilises a polyclonal capture antibody coated to polystyrene beads and acridinium ester-labelled human lysozyme as tracer. Samples are incubated with polystyrene beads and tracer overnight at 4 degrees C. After a thorough washing step, emitted light is measured by an automated luminometer for 2 seconds. The standard curve uses five standards ranging from 0.025 to 6.4 mg/l. The method has a sensitivity of 0.02 mg/l. Dilution recoveries for three samples were 88, 104 and 108%. Intraassay coefficients of variation (CV, n = 24) were 10.1% and 11.7% for a healthy control and a patient sample; interassay CV (n = 16) were 6.7% and 13.1% for the same healthy control but another patient sample. The normal range of faecal lysozyme in 80 healthy controls was found to be 0.02-1 mg/l (97.5 percentile) with a median of 0.28 mg/l. Fifty-three patients with Crohn's disease had faecal lysozyme values ranging from 0.16 to 100.7 mg/l with a median of 1.75 mg/l, and 30 patients with ulcerative colitis showed levels between 0.09 and 118 mg/l with a median of 1.11 mg/l. The assay has proved useful for differentiating healthy individuals from those with inflammatory bowel disease and might be a valuable tool for diagnosing or evaluating inflammatory bowel disease.

Publication types

  • Clinical Trial

MeSH terms

  • Adolescent
  • Adult
  • Aged
  • Aged, 80 and over
  • Child
  • Colitis, Ulcerative / diagnosis
  • Colitis, Ulcerative / enzymology
  • Crohn Disease / diagnosis
  • Crohn Disease / enzymology
  • Diagnosis, Differential
  • Feces / enzymology*
  • Female
  • Humans
  • Immunoglobulin G / analysis
  • Indicators and Reagents
  • Isotope Labeling
  • Luminescent Measurements
  • Male
  • Middle Aged
  • Muramidase / analysis*
  • Radioimmunoassay
  • Reference Values

Substances

  • Immunoglobulin G
  • Indicators and Reagents
  • Muramidase