Molecular determinants of high affinity dihydropyridine binding in L-type calcium channels

J Biol Chem. 1996 Mar 8;271(10):5293-6. doi: 10.1074/jbc.271.10.5293.

Abstract

The pore-forming alpha1 subunit of L-type voltage-gated Ca2+ channels is pharmacologically modulated by dihydropyridine (DHP) Ca2+ antagonists and agonists. Site-directed mutation of amino acids within transmembrane segments IIIS6 and IVS6 to those characteristic of DHP-insensitive channels revealed 2 mutations in IIIS6 (I1049F and I1052F) and 4 mutations in IVS6 (Y1365I, M1366F, I1372M, and I1373L) with increased KD values for (+)-[3H]PN200-110 binding. A tyrosine residue (Y1048) in IIIS6 that is conserved between DHP-sensitive and -insensitive Ca2+ channels was also altered by mutagenesis. Y1048F had a KD for (+)-[3H]PN200-110 binding that was increased 12-fold, and Y1048A had a KD at least 1000-fold higher than that of wild-type. These results support the hypothesis that transmembrane segments IIIS6 and IVS6 both contribute critical amino acid residues to the DHP receptor site and that Tyr-1048 within transmembrane segment IIIS6 is required for high affinity DHP binding, even though it is conserved between DHP-sensitive and -insensitive Ca2+ channels.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Binding Sites
  • Binding, Competitive
  • Calcium Channel Blockers / metabolism
  • Calcium Channels / chemistry
  • Calcium Channels / metabolism*
  • Calcium Channels, L-Type
  • Cloning, Molecular
  • Dihydropyridines / metabolism*
  • Isradipine / metabolism
  • Kinetics
  • Macromolecular Substances
  • Models, Structural
  • Molecular Sequence Data
  • Muscle, Skeletal / metabolism
  • Mutagenesis, Site-Directed
  • Point Mutation
  • Protein Structure, Secondary
  • Rabbits
  • Radioligand Assay
  • Recombinant Proteins / metabolism
  • Structure-Activity Relationship
  • Tritium

Substances

  • Calcium Channel Blockers
  • Calcium Channels
  • Calcium Channels, L-Type
  • Dihydropyridines
  • Macromolecular Substances
  • Recombinant Proteins
  • Tritium
  • 1,4-dihydropyridine
  • Isradipine